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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1018071Erstellt: 24. Oktober 2026

Benzoyl Peroxide → 1-Butanone, 1-[4-(1-bromo-1-methylethyl)phenyl]-4-chloro-

https://huagongshe.com/de/reaction/1018071

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzoyl PeroxideHCID 7187—
EduktN-bromobutanimideHCID 67184—
Edukt4-Chloro-4'-isopropylbutyrophenoneHCID 98744—
LösungsmittelCarbon TetrachlorideHCID 5943—
Produkt1-Butanone, 1-[4-(1-bromo-1-methylethyl)phenyl]-4-chloro-HCID 10063579—

Reaktionsschritte

Dissolve 4-chloro-1-(4-isopropyl-phenyl)-butan-1-one (2.10 g, 9.35 mmol) in carbontetrachloride (30 mL), add N-bromosuccinimide (1.75 g, 9.83 mmol) and benzoylperoxide (3 mg) and stir at reflux for 1 hour. Cool the reaction mixture, filter, wash with water and brine. Dry (MgSO4), filter and vaporate the solvent in vacuo to give the title compound as an amber oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06479663B2
Quelldatensatzuspto-grants-2002_11
ORD IDord-0da1afb1fa93436892c181bd0e74b94f
Quellennotizuspto-grants-2002_11