HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
tert-Butanol → HCID 86745735, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | tert-Butanol | HCID 6386 | — |
| Edukt | Methyl Decanoate | HCID 8050 | — |
| Edukt | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 86745735 | HCID 86745735 | — |
Reaktionsschritte
25 ml of tertiary butanol was added to a mixture of 5.00 g (27.64 mM) of glucose and 1.03 g (5.55 mM) of methyl caprinate, and 100 mg of thermostable lipase derived from Candida antarctica (sp-382, manufactued by NOVO Co.) immobilized into an acrylic resin was further added. Then, they were refluxed under heating while stirring for 24 hours with an addition of 10 g of molecular sieves 5A as a methanol remover, to obtain glucose monocaprinate (C10 glucose ester).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05109127 |
| Quelldatensatz | uspto-grants-1992_04 |
| ORD ID | ord-344f50ca68b04784888a853a933057d8 |
| Quellennotiz | uspto-grants-1992_04 |