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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1031224Erstellt: 24. Oktober 2026

tert-Butanol → HCID 86745735, Verbindung

https://huagongshe.com/de/reaction/1031224

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukttert-ButanolHCID 6386—
EduktMethyl DecanoateHCID 8050—
Edukt(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanalHCID 107526—
LösungsmittelMethanolHCID 887—
ProduktHCID 86745735HCID 86745735—

Reaktionsschritte

25 ml of tertiary butanol was added to a mixture of 5.00 g (27.64 mM) of glucose and 1.03 g (5.55 mM) of methyl caprinate, and 100 mg of thermostable lipase derived from Candida antarctica (sp-382, manufactued by NOVO Co.) immobilized into an acrylic resin was further added. Then, they were refluxed under heating while stirring for 24 hours with an addition of 10 g of molecular sieves 5A as a methanol remover, to obtain glucose monocaprinate (C10 glucose ester).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05109127
Quelldatensatzuspto-grants-1992_04
ORD IDord-344f50ca68b04784888a853a933057d8
Quellennotizuspto-grants-1992_04