Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 3-(2-Methylpropenyl)benzonitrile | HCID 19024792 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 3-Isobutylbenzonitrile | HCID 19024755 | 94% |
Reaktionsschritte
To a solution of 3-(2-methyl-1-propenyl)benzonitrile (5.80 g) in methanol (50 ml) was added 10% palladium on activated carbon (1 g), and the mixture was stirred under hydrogen atmosphere (3 atm) at 25° C. for 1 hour. The catalyst was filtered off and the liltrate was evaporated to give 3-isobutylbenzonitrile (5.52 g) as a pale yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05312829 |
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| Quelldatensatz | uspto-grants-1994_05 |
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| ORD ID | ord-f5fee2c5150e427682aeaa078f4e5058 |
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| Quellennotiz | uspto-grants-1994_05 |
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