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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1041821Erstellt: 24. Oktober 2026

1,2-Dichloroethane → 6-Amino-2-[bis(carboxymethyl)amino]hexanoic acid

https://huagongshe.com/de/reaction/1041821

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,2-DichloroethaneHCID 11—
EduktN-(5-Amino-1-carboxypentyl)iminodiacetic acidHCID 7019830—
LösungsmittelDimethyl SulfoxideHCID 679—
Produkt6-Amino-2-[bis(carboxymethyl)amino]hexanoic acidHCID 2735296—

Reaktionsschritte

A solution was prepared by the addition of 1 mmol of EDC and 0.2 mmol of NHS to 1 ml of DMSO, and 50 μl of the thus prepared solution was added onto the CMD film. The solution was then allowed to undergo the reaction at the room temperature for 30 minutes. After the solution was removed, washing with DMSO was performed one time. Also, a solution prepared by the addition of 0.1 mmol of AB-NTA (supplied by Dojin Kagaku K.K.) to 1 ml of DMSO was allowed to undergo the reaction for 12 hours. The solution was removed, and washing with ultra pure water was performed one time.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08557194B2
Quelldatensatzuspto-grants-2013_10
ORD IDord-875e695d231845f9836da25fe77b3704
Quellennotizuspto-grants-2013_10