HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4,5-Dichlorophthalic anhydride → Ethyl 3-(5,6-dichloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4,5-Dichlorophthalic anhydride | HCID 70334 | — |
| Edukt | Ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982228 | — |
| Produkt | Ethyl 3-(5,6-dichloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982181 | — |
Reaktionsschritte
Ethyl 3-(5,6-dichloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared (0.66 g, 50%) in the same manner as described in the above example 5 (20) from ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (0.60 g, 3.25 mmol) and 4,5-dichlorophthalic anhydride (0.85 g, 3.90 mmol), and the obtained product was identified with the following NMR data.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07094908B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-b65c8bbe15784ca3b285bbca9b865f1d |
| Quellennotiz | uspto-grants-2006_08 |