HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenylmaleic anhydride → Ethyl 3-(2,5-dioxo-3-phenyl-2,5-dihydro-pyrrol-1-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenylmaleic anhydride | HCID 99174 | — |
| Edukt | Ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982228 | — |
| Produkt | Ethyl 3-(2,5-dioxo-3-phenyl-2,5-dihydro-pyrrol-1-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982270 | — |
Reaktionsschritte
Ethyl 3-(2,5-dioxo-3-phenyl-2,5-dihydro-pyrrol-1-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared (0.41 g, 58%) in the same manner as described in the above example 5 (20) from ethyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (0.40 g, 1.96 mmol) and phenylmaleic anhydride (0.57 g, 2.16 mmol), and the obtained product was identified with the following NMR data.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07094908B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-add2ac49407c438e8ea33308f273e188 |
| Quellennotiz | uspto-grants-2006_08 |