Diethyl Ether → N-(4-Benzyloxybenzyl)-N-(t-butylcarbonyloxy)acetamide

Beteiligte Stoffe

Reaktionsschritte

Pivaloylchloride (1.36 ml) was added dropwise to a solution of N-(4-benzyloxybenzyl)acetohydroxamic acid (2.71 g) and triethylamine (1.7 ml) in methylene dichloride (15 ml) and dimethylaminopyridine (100 ml). The mixture was stirred for 2 hours at room temperature, then neutral material was isolated with ether. The product, N-(4-(Benzyloxybenzyl)-N-(t-butylcarbonyloxy)acetamide, was a colourless oil.

Herkunft & Nachweise