HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid → methyl N-propyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)-2-pyrrolecarboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid | HCID 19694676 | — |
| Edukt | methyl N-propyl-4-iodo-2-pyrrolecarboxylate | HCID 19694682 | — |
| Produkt | methyl N-propyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)-2-pyrrolecarboxylate | HCID 19694683 | 22,3% |
Reaktionsschritte
Following the basic procedure of Example 7(f), by reacting 1.7 g (6 mmol) of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthrylboronic acid with 1.47 g (5 mmol) of methyl N-propyl-4-iodo-2-pyrrolecarboxylate, 450 mg (22%) of methyl N-propyl-4-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-anthryl)-2-pyrrolecarboxylate were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05723499 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-00a204d0f65b435cab8a71dca632e9c7 |
| Quellennotiz | uspto-grants-1998_03 |