HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(Diethylamino)-1-propanol → Diethyl-[3-(2-fluoro-4-nitro-phenoxy)-propyl]-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(Diethylamino)-1-propanol | HCID 12159 | — |
| Edukt | 1,2-Difluoro-4-nitrobenzene | HCID 123053 | — |
| Produkt | Diethyl-[3-(2-fluoro-4-nitro-phenoxy)-propyl]-amine | HCID 21974931 | — |
Reaktionsschritte
In a manner similar to that described in Example 231a, 3,4-difluoronitrobenzene (6.7 mL, 60.6 mmol, 1 equiv.) and 3-diethylamino-1-propanol (9 mL, 1 equiv.) are converted to the named compound as a brown oil (16.3 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07098236B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-56b3fcc70da64331a887512e770547de |
| Quellennotiz | uspto-grants-2006_08 |