HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Phenethylamine → 1-Phenethylamine, (+)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Phenethylamine | HCID 7408 | — |
| Edukt | (R)-(-)-2-propyloctanoic acid | HCID 208925 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 1-Phenethylamine, (+)- | HCID 643189 | 88,2% |
Reaktionsschritte
Using the crystal comprising (2R)-2-propyloctanoic acid and R)-(+)-1-phenylethylamine (6.8 g) produced in the second recrystallization and acetonitrile (102 mL), the same operation as in the second recrystallization was made to give the crystal comprising (2R)-2-propyloctanoic acid and (R)-(+)-1-phenylethylamine (6.0 g, 98.9% e.e.; yield 88%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07820715B2 |
| Quelldatensatz | uspto-grants-2010_10 |
| ORD ID | ord-54191d2ebb5b469a828f5070eff5df6b |
| Quellennotiz | uspto-grants-2010_10 |