HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-hydroxymethyl-pyrazol-1-yl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Edukt | 1-Hydroxy-4-hydroxymethylpyrazole | HCID 22047685 | — |
| Produkt | Methyl-phenyl-carbamic Acid 4-hydroxymethyl-pyrazol-1-yl Ester | HCID 69517970 | — |
Reaktionsschritte
The title compound was prepared from 1-hydroxy-4-hydroxymethylpyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (62%, oil).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07279470B2 |
| Quelldatensatz | uspto-grants-2007_10 |
| ORD ID | ord-e590bc1a1fcb455e8b7025df7a0801c1 |
| Quellennotiz | uspto-grants-2007_10 |