HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetonitrile → HCID 178470380, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetonitrile | HCID 6342 | — |
| Edukt | 1-Naphthalenemethanamine | HCID 8355 | — |
| Edukt | Ethyl 2,3-dioxobutanoate | HCID 12260829 | — |
| Produkt | HCID 178470380 | HCID 178470380 | — |
Reaktionsschritte
A solution of 2,3-dioxobutyric acid ethyl ester, (Z)-2-oxime (3 g), 1-naphthalenemethylamine (3.26 g) in acetonitrile (45 ml) is refluxed for 10 hr to give a white precipitate. The solid is then collected, washed with acetonitrile and dried to yield 5-methyl-2-naphthalen-1-yl-3H-imidazole-4-carboxylic acid ethyl ester. LCMS 281.3 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07728009B1 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-3f58c3e8254649fcb1cc5fa9783b5209 |
| Quellennotiz | uspto-grants-2010_06 |