HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Imidazole → Bis-(1H-imidazol-2-YL)-methanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Imidazole | HCID 795 | — |
| Edukt | Triphosgene | HCID 94429 | — |
| Produkt | Bis-(1H-imidazol-2-YL)-methanone | HCID 5250894 | — |
| Produkt | Imidazolium chloride | HCID 10197644 | — |
Reaktionsschritte
Reaction of imidazole with bis (trichloromethyl) carbonate produces carbonyl diimidazole and crystalline imidazole hydrochloride. Insoluble imidazole hydrochloride is removed from the reaction mixture quantitatively by filtration and the carbonyl diimidazole is recovered by removing the solvent or crystallization under cooling or a combination thereof.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06455702B1 |
| Quelldatensatz | uspto-grants-2002_09 |
| ORD ID | ord-f734730a142b45d28a7983dd411b3709 |
| Quellennotiz | uspto-grants-2002_09 |