HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Naphthoyl chloride → 3-{4-[(Naphthalene-2-carbonyl)-amino]-phenyl)-acrylic acid methyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Naphthoyl chloride | HCID 75246 | — |
| Edukt | 2-Propenoic acid, 3-(4-aminophenyl)-, methyl ester | HCID 3017578 | — |
| Produkt | 3-{4-[(Naphthalene-2-carbonyl)-amino]-phenyl)-acrylic acid methyl ester | HCID 66958345 | — |
Reaktionsschritte
Using an analogous method (H4), the title compound was prepared from 2-naphthalenecarbonyl chloride (0.557 g, 2.91 mmol) and 3-(4-amino-phenyl)-acrylic acid methyl ester (3) in a form of white solid (0.950 g, 75%). 1H NMR (DMSO-d6, HMDSO), δ: 3.65 (3H, s); 6.51 (1H, d, J=16.0 Hz); 7.47-8.25 (12H, m); 10.63 (1H, s).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07880020B2 |
| Quelldatensatz | uspto-grants-2011_02 |
| ORD ID | ord-94d7b429993b4eb68202734b1cc6d13d |
| Quellennotiz | uspto-grants-2011_02 |