HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Chlorophenyl chloroformate → 2-Chlorophenyl 4-(prop-2-ynyl)piperidine-1-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Chlorophenyl chloroformate | HCID 4184068 | — |
| Edukt | Tert-butyl 4-(prop-2-yn-1-yl)piperidine-1-carboxylate | HCID 18187546 | — |
| Produkt | 2-Chlorophenyl 4-(prop-2-ynyl)piperidine-1-carboxylate | HCID 57838891 | — |
Reaktionsschritte
2-(chloro)phenyl chloroformate (5.00 g, 26.2 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (4.50 g, 20.2 mmol) according to general procedure 1. Yield=4.56 g, 82%. m/z MH+=278.13. HPLC rt=9.3 min.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07888329B2 |
| Quelldatensatz | uspto-grants-2011_02 |
| ORD ID | ord-8b8bbe6a4ba54c138065b16c64258669 |
| Quellennotiz | uspto-grants-2011_02 |