HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
methyl 2-amino-1H-benzo[d]imidazole-4-carboxylate → 2-amino-6-pyridin-4-yl-1H-benzoimidazole-4-carboxylic acid methyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | methyl 2-amino-1H-benzo[d]imidazole-4-carboxylate | HCID 24730367 | — |
| Edukt | HCID 66940533 | HCID 66940533 | — |
| Produkt | 2-amino-6-pyridin-4-yl-1H-benzoimidazole-4-carboxylic acid methyl ester | HCID 66940503 | 50% |
Reaktionsschritte
0.25 g (50% overall yield) of 2-amino-6-pyridin-4-yl-1H-benzoimidazole-4-carboxylic acid methyl ester was synthesized according to procedures described for the synthesis of 2-Amino-1H-benzoimidazole-4-carboxylic acid methyl ester (intermediate A) starting from 0.5 g (1.8 mmol) of above synthesized 2-Amino-3-nitro-5-pyridin-4-yl-benzoic acid methyl ester. LCMS: 269 (M+1)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07893267B2 |
| Quelldatensatz | uspto-grants-2011_02 |
| ORD ID | ord-94de602cfd914badaabf1906ea619415 |
| Quellennotiz | uspto-grants-2011_02 |