HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dithiodibenzoic acid → 2,2'-Dithiobis[n-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamide]
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dithiodibenzoic acid | HCID 8409 | — |
| Edukt | Tricyclo(3.3.1.13,7)dec-1-ylmethylamine | HCID 86625 | — |
| Katalysator | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Produkt | 2,2'-Dithiobis[n-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)-benzamide] | HCID 88163524 | 30,6% |
Reaktionsschritte
Prepared according to the method of Example 14 from 1-adamantanemethylamine (0.23 g), 4-dimethylaminopyridine (0.006 g) and 2,2′dithiosalicylic acid (0.2 g) to give the sub-title compound as an off-white solid (0.12 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06258838B1 |
| Quelldatensatz | uspto-grants-2001_07 |
| ORD ID | ord-d2fd3b4931a34f3a890ac3cd8b1f85fc |
| Quellennotiz | uspto-grants-2001_07 |