Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1-Propanol | HCID 1031 | — |
| Edukt | Ferulic Acid | HCID 445858 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | n-Propyl ferulate | HCID 9881169 | 64,3% |
Reaktionsschritte
In a three-necked flask, 19.4 g (0.1 mole) of ferulic acid, 6.01 g (0.1 mole) of n-propyl alcohol, and 1.0 g of paratoluenesulfonic acid were placed, and 200 ml of benzene was added. This reaction mixture was stirred at 78° C. for 15 hours. Thereafter, the same procedures were taken as in Example 1 to obtain 15.2 g (yield: 64%) of n-propyl ferulate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05908615 |
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| Quelldatensatz | uspto-grants-1999_06 |
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| ORD ID | ord-15ba7c8842c246b2ba780fbfe5aa43cf |
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| Quellennotiz | uspto-grants-1999_06 |
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