HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Iodine → 2-[2-(Diethylamino)ethyl]-6-phenyl-isothiazolo[5,4-d]pyrimidin-3(2H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Iodine | HCID 807 | — |
| Edukt | HCID 178418472 | HCID 178418472 | — |
| Produkt | 2-[2-(Diethylamino)ethyl]-6-phenyl-isothiazolo[5,4-d]pyrimidin-3(2H)-one | HCID 9905503 | 68,5% |
Reaktionsschritte
Using the procedure of Example 20, 3.3 g (0.01 mol) of 4-mercapto-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide (from Preparation 36) and 2.54 g (0.01 mol) of iodine were reacted to give 2.25 g of the title compound after recrystallization from isopropanol, mp 106°-107° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05889034 |
| Quelldatensatz | uspto-grants-1999_03 |
| ORD ID | ord-bf5358c4af08405b818719f715aef401 |
| Quellennotiz | uspto-grants-1999_03 |