Hydrochloric Acid → Methyl 4-benzyloxybenzimidate hydrochloride

Beteiligte Stoffe

Reaktionsschritte

A solution of 560 mg of 4-benzyloxybenzonitrile in 16 ml of THF and 0.2 ml of methanol, cooled to 0° C., was saturated with hydrogen chloride and kept at 4° C. for 16 hours. The precipitate was filtered off, washed with diethyl ether and dried to give 357 mg of methyl 4-benzyloxybenzimidate hydrochloride, m.p. 179°-180° C.

Herkunft & Nachweise