HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanolamine → N-(2-hydroxyethyl)-aminobutyric acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanolamine | HCID 700 | — |
| Edukt | Crotonic Acid | HCID 637090 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | N-(2-hydroxyethyl)-aminobutyric acid | HCID 18780751 | — |
Reaktionsschritte
A solution of 86 g of crotonic acid (1 mole) and ethanolamine (1 mole) in pyridine (200 ml) is refluxed for 2-3 hours and subsequently cooled. The resulting product is filtered and recrystallized to yield the title compound having m.p. 178-180° C. (Compound 1.1, Table 1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06075051 |
| Quelldatensatz | uspto-grants-2000_06 |
| ORD ID | ord-b731145f17b94acfbc45469dfbb0a26a |
| Quellennotiz | uspto-grants-2000_06 |