HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dimethylbenzoic acid → 3,4-dimethyl-N-(5-methylhexan-3-yl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dimethylbenzoic acid | HCID 12073 | — |
| Edukt | 5-Methylhexan-3-amine | HCID 22955496 | — |
| Produkt | 3,4-dimethyl-N-(5-methylhexan-3-yl)benzamide | HCID 57527902 | — |
Reaktionsschritte
Prepared in a similar manner to example 4 using 3,4-dimethylbenzoic acid and 5-methylhexan-3-amine (example 5a). 1H NMR (500 MHz, CDCl3): δ 0.94 (m, 9H); 1.38 (m, 2H); 1.46 (m, 1H); 1.65 (m, 2H); 2.29 (s, 3H); 2.30 (s, 3H); 4.18 (m, 1H); 5.70 (d, 1H); 7.17 (d, 1H); 7.46 (d, 1H); 7.55 (s, 1H). MS (248, M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07476399B2 |
| Quelldatensatz | uspto-grants-2009_01 |
| ORD ID | ord-6cfe2c2000484a17823b88dae33d8fff |
| Quellennotiz | uspto-grants-2009_01 |