HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phosphorus oxychloride → 1-Allyl-2-(2-morpholinophenyl)-1,3,3-trimethylguanidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phosphorus oxychloride | HCID 24813 | — |
| Edukt | 2-Morpholinoaniline | HCID 735756 | — |
| Edukt | 3-Allyl-1,1,3-trimethylurea | HCID 18952316 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | 1-Allyl-2-(2-morpholinophenyl)-1,3,3-trimethylguanidine | HCID 15746402 | — |
Reaktionsschritte
Reaction of 3-allyl-1,1,3-trimethylurea (7.17 g) in benzene (50 ml) with 4-(2-aminophenyl)morpholine (6 g) in benzene (30 ml) in the presence of phosphorus oxychloride (4.71 ml) for 45 hours at 70° C. gave 1-allyl-2-(2-morpholinophenyl)-1,3,3-trimethylguanidine (bp. 148°-150° C. at 0.2 mm Hg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05373008 |
| Quelldatensatz | uspto-grants-1994_12 |
| ORD ID | ord-0607a0d79f4745e199209c9667db503e |
| Quellennotiz | uspto-grants-1994_12 |