HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 15741Erstellt: 24. Oktober 2026
Dimethylformamide dimethyl acetal → Ethyl 1-(4-chlorophenylsulfonyl)-3-((dimethylamino)methylene)-4-oxo-1,2,3,4-tetrahydropyridine-2-carboxylate
https://huagongshe.com/de/reaction/15741
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Edukt | Ethyl 1-(4-chlorophenylsulfonyl)-4-oxo-1,2,3,4-tetrahydropyridine-2-carboxylate | HCID 59342383 | — |
| Produkt | Ethyl 1-(4-chlorophenylsulfonyl)-3-((dimethylamino)methylene)-4-oxo-1,2,3,4-tetrahydropyridine-2-carboxylate | HCID 68502343 | — |
Reaktionsschritte
Compound 103 (5.0 g, 15 mmol) was dissolved in DMF-DMA (20 mL) and heated at 100° C. for 30 minutes. The reaction mixture was concentrated in vacuo to yield compound 104 as a yellow oil that was used without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US07732609B2 |
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| Quelldatensatz | uspto-grants-2010_06 |
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| ORD ID | ord-916c1a439c9a48dfb8e5e3b3454c7fcd |
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| Quellennotiz | uspto-grants-2010_06 |
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