HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sulfuric Acid → Anthraquinone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | Purpurin anthraquinone | HCID 6683 | — |
| Edukt | N-Methylolacrylamide | HCID 13543 | — |
| Produkt | Anthraquinone | HCID 6780 | — |
Reaktionsschritte
Twenty-five parts of 1,2,4-trihydroxy-anthraquinone was added to 45 parts of concentrated sulfuric acid. The obtained mixture was cooled with ice in a nitrogen atmosphere. Then, 15 parts of N-methylolacrylamide was added to the resulting mixture in portions. After the completion of the addition, the obtained mixture was stirred at room temperature for 24 hours and poured over a large amount of ice. The precipitate thus formed was recrystallized from ethanol to give a reddish-brown polymerizable anthraquinone dye F. The anthraquinone dye F is represented by the below chemical formula (VII). ##STR7##
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05942292 |
| Quelldatensatz | uspto-grants-1999_08 |
| ORD ID | ord-6ad16c9d725f4e9a9ebec3519a1d67b4 |
| Quellennotiz | uspto-grants-1999_08 |