HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetaldehyde → Quindoxin
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetaldehyde | HCID 177 | — |
| Edukt | Benzofuroxan | HCID 68075 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | Quindoxin | HCID 72073 | — |
Reaktionsschritte
A mixture of benzofuroxan (2.5 g.), acetaldehyde (2.5 ml.) and triethylamine (20 ml.) is allowed to stand at room temperature for 24 hours. The solid material which precipitates is filtered and dried to give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04866175 |
| Quelldatensatz | uspto-grants-1989_09 |
| ORD ID | ord-8ce7d3dd4f95463ab3b62df2f02df71b |
| Quellennotiz | uspto-grants-1989_09 |