Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 3-Pyridinemethanamine | HCID 31018 | — |
| Edukt | 6-Methoxyphthalide | HCID 330539 | — |
| Produkt | HCID 20082005 | HCID 20082005 | 91,8% |
Reaktionsschritte
A mixture of 919 mg of 6-methoxyisobenzofuran-1 (3H)-one and 1.82 g of 3-aminomethylpyridine was heated at 150° C. without solvent for 3 hours under stirring. After finishing the reaction, the mixture was chromatographed on a column of silica gel, eluting with ethyl acetate and then with tetrahydrofuran to give 1.40 g of the titled compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05401756 |
|---|
| Quelldatensatz | uspto-grants-1995_03 |
|---|
| ORD ID | ord-c962d1214f004a7bb3220bdf4e352a35 |
|---|
| Quellennotiz | uspto-grants-1995_03 |
|---|
