Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Nitrobenzene | HCID 7416 | — |
| Edukt | Tetramethylammonium hydroxide dihydrate | HCID 22116808 | — |
| Lösungsmittel | Benzonitrile | HCID 7505 | — |
| Produkt | Azoxybenzene | HCID 10316 | 45% |
Reaktionsschritte
A solution containing 10 g of nitrobenzene, 1.27 g of tetramethylammonium hydroxide dihydrate and 1 g of benzonitrile was stirred at 60° C. with nitrogen bubbled into the solution via a syringe needle for 1 hour. Analysis of a sample of the reaction product by HPLC revealed N-(4-nitrophenyl)-benzamide was produced in 45% yield and azoxybenzene was generated in 22% yield based on tetramethylammonium hydroxide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05436371 |
|---|
| Quelldatensatz | uspto-grants-1995_07 |
|---|
| ORD ID | ord-8c37f1219c634a3799c46187d1f88a83 |
|---|
| Quellennotiz | uspto-grants-1995_07 |
|---|
