HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1658263Erstellt: 24. Oktober 2026
O-Xylene → alpha-(2-Imidazolin-2-ylaminomethyl)-p-methylbenzyl alcohol
https://huagongshe.com/de/reaction/1658263
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | O-Xylene | HCID 7237 | — |
| Edukt | 2-Nitroamino-2-imidazoline | HCID 410042 | — |
| Edukt | 2-Amino-1-(4-methylphenyl)ethan-1-ol | HCID 3519929 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | alpha-(2-Imidazolin-2-ylaminomethyl)-p-methylbenzyl alcohol | HCID 53928717 | — |
Reaktionsschritte
A mixture of 9.06 parts of α-(aminomethyl)-p-methylbenzyl alcohol, 7.8 parts of 2-(nitramino)-2-imidazoline and 8 parts of xylene is stirred for 30 minutes at 160°C (oil-bath). The reaction mixture is cooled and acetone is added. The precipitated product is filered off, washed with acetone and dried, yielding α-(2-imidazolin-2-ylaminomethyl)-p-methylbenzyl alcohol; 163.7°C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US03963718 |
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| Quelldatensatz | uspto-grants-1976_06 |
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| ORD ID | ord-4a3df0ece58b4090bbea5a90636fa23a |
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| Quellennotiz | uspto-grants-1976_06 |
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