HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclohexylamine, 2-phenyl-, hydrochloride, trans- → N-[(1R,2S)-2-phenylcyclohexyl]azepan-2-imine;hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclohexylamine, 2-phenyl-, hydrochloride, trans- | HCID 209556 | — |
| Edukt | rac-(1R,2R)-2-phenylcyclopentan-1-amine hydrochloride | HCID 70051154 | — |
| Produkt | N-[(1R,2S)-2-phenylcyclohexyl]azepan-2-imine;hydrochloride | HCID 145795666 | — |
Reaktionsschritte
Following the procedure of Example 1, only substituting for cis-2-phenylcyclopentylamine hydrochloride an appropriate amount of trans-2-phenylcyclohexylamine hydrochloride, M.P. 251°-257° C., and employing a reaction time of 38 days, the desired product was obtained, M.P. 236°-239° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04126613 |
| Quelldatensatz | uspto-grants-1978_11 |
| ORD ID | ord-70830adb200b4ce6864777b04bb5b02c |
| Quellennotiz | uspto-grants-1978_11 |