HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(3-(Prop-1-en-2-yl)phenyl)propan-2-amine → 1-Methyl-1-[3-(1-methylethyl)phenyl]ethylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(3-(Prop-1-en-2-yl)phenyl)propan-2-amine | HCID 14716541 | — |
| Katalysator | Platinum oxide (PtO) | HCID 82844 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1-Methyl-1-[3-(1-methylethyl)phenyl]ethylamine | HCID 20811513 | 97,7% |
Reaktionsschritte
First, 0.5 g of platinum oxide was added to a solution formed by dissolving 25.3 g of 1-methyl-1-[3-(1-methylethenyl)phenyl]ethylamine in 100 ml of ethyl alcohol, and a hydrogenation reaction was then carried out at a temperature of 15° to 35° C. for 7 hours under atmospheric pressure under a hydrogen gas stream. Afterward, reaction residues were removed by filtration, and the resultant filtrate was then concentrated to obtain 25.0 g of 1-methyl-1-[3-(1-methylethyl)phenyl]ethylamine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05352655 |
| Quelldatensatz | uspto-grants-1994_10 |
| ORD ID | ord-7a6cb0e023ff424598a8b15998185638 |
| Quellennotiz | uspto-grants-1994_10 |