HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Aminophenol → HCID 23106862, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Aminophenol | HCID 5801 | — |
| Edukt | 2-Iodohexane | HCID 33019 | — |
| Produkt | HCID 23106862 | HCID 23106862 | — |
Reaktionsschritte
The same procedure as in Example 6 was repeated except that the molar ratio of 2-iodohexane to o-aminophenol was changed to 0.8, the 2-iodohexane was dropped over 4.5 h, and then the reaction mixture was stirred at room temperature for 0.5 h. As a result, it was confirmed that the rate of conversion of o-aminophenol was 71%, the selectivity to the N-monoalkylated compound was 86%, and the oxygen absorption initiation time as an index of determining an oxidation-inhibiting property thereof was 320 min.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07498467B2 |
| Quelldatensatz | uspto-grants-2009_03 |
| ORD ID | ord-25de0d922c614920bc11e2d755fc570c |
| Quellennotiz | uspto-grants-2009_03 |