HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetaldehyde → 4-Trifluoromethyl-7-methyl-6-ethyl-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetaldehyde | HCID 177 | — |
| Edukt | 4-Trifluoromethyl-7-methyl-6-cyclopropylmethyl-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one | HCID 9967568 | — |
| Produkt | 4-Trifluoromethyl-7-methyl-6-ethyl-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one | HCID 9901266 | — |
Reaktionsschritte
This compound was prepared in a similar fashion as that described in Example 84 from Compound 187 (Structure 33 of Scheme VI, where R1=methyl, n=1) and acetaldehyde. 1H NMR (400 MHz, CDCl3) 11.19 (br. s, 1H), 7.11 (s, 1H), 7.00 (s, 1H), 6.80 (s, 1H), 3.55 (m, 1H), 3.47–3.32 (m, 2H), 2.93–2.80 (m, 2H), 1.93–1.79 (m, 2H), 1.22 (t, 3H, J=7.0), 1.18 (d, 3H, J=6.4).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07026484B2 |
| Quelldatensatz | uspto-grants-2006_04 |
| ORD ID | ord-c3a9531e41324bec9ec80d4b8c222eda |
| Quellennotiz | uspto-grants-2006_04 |