HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol, 1-ethoxy-2,2,2-trifluoro- → 4-Trifluoromethyl-6-(2,2,2-trifluoroethyl)-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol, 1-ethoxy-2,2,2-trifluoro- | HCID 9897 | — |
| Edukt | 4-Trifluoromethyl-7-methyl-6-(2,2,2-trifluoroethyl)-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one | HCID 10270119 | — |
| Produkt | 4-Trifluoromethyl-6-(2,2,2-trifluoroethyl)-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one | HCID 10154869 | — |
Reaktionsschritte
This compound was prepared in a similar fashion as that described in Example 84 from Compound 192 (Structure 33 of Scheme VI, where R1=H, n=1) and trifluoroacetaldehyde ethyl hemiacetal. 1H NMR (400 MHz, CDCl3) 11.32 (br. s, 1H), 7.11 (s, 1H), 7.02 (s, 1H), 6.99 (s, 1H), 3.88 (q, 2H, J=8.9), 3.47 (t, 2H, J=5.6), 2.93 (t, 2H, J=6.3), 2.03 (m, 2H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07026484B2 |
| Quelldatensatz | uspto-grants-2006_04 |
| ORD ID | ord-51646d06e7ac417ab0c42bc6c479963e |
| Quellennotiz | uspto-grants-2006_04 |