Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1840941Erstellt: 24. Oktober 2026

Tert-butyl 4-(benzyloxy)benzoate → tert-Butyl 4-hydroxybenzoate

https://huagongshe.com/de/reaction/1840941

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTert-butyl 4-(benzyloxy)benzoateHCID 53864121—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
Produkttert-Butyl 4-hydroxybenzoateHCID 11764095%

Reaktionsschritte

0.36 g of 10% palladium on activated carbon were added to a solution of 1.2 g (4.3 mmol) of 4-benzyloxy-benzoic acid tert-butyl ester in 45 mL of ethanol and this mixture was hydrogenated at 20 psi for 3 hours. After filtering over celite and removing the solvent under reduced pressure 0.79 g (95% yield) of 4-hydroxy-benzoic acid tert-butyl ester were obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06683096B2
Quelldatensatzuspto-grants-2004_01
ORD IDord-088307d29382438e849941b901475049
Quellennotizuspto-grants-2004_01