HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Chloropyridine-2-carboxylic acid → HCID 178522734, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Chloropyridine-2-carboxylic acid | HCID 824632 | — |
| Edukt | HCID 178509299 | HCID 178509299 | — |
| Lösungsmittel | Thionyl Chloride | HCID 24386 | — |
| Produkt | HCID 178522734 | HCID 178522734 | 39,3% |
Reaktionsschritte
0.53 g of 3-chloro-2-pyridinecarboxylic acid, 10 ml of thionyl chloride and 0.27 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and ethanol, whereby 0.28 g of N-(5-tetrazolyl)-3-chloro-2-pyridinecarboxamide is obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04404214 |
| Quelldatensatz | uspto-grants-1983_09 |
| ORD ID | ord-506cde04188f4f70be64ab4491622625 |
| Quellennotiz | uspto-grants-1983_09 |