HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2048249Erstellt: 24. Oktober 2026
Ethyl 2-[(2'-cyanobiphenyl-4-yl)methyl]-3-oxohexanoate → HCID 67008513, Verbindung
https://huagongshe.com/de/reaction/2048249
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Ethyl 2-[(2'-cyanobiphenyl-4-yl)methyl]-3-oxohexanoate | HCID 10020734 | — |
| Edukt | HCID 178489584 | HCID 178489584 | — |
| Produkt | HCID 67008513 | HCID 67008513 | 46% |
Reaktionsschritte
A mixture of ethyl 2-[(2′-cyanobiphenyl-4-yl)methyl]-3-oxohexanoate (0.83 g) and N-(2-methoxycyclohexyl)-5-methyl-4H-1,2,4-triazol-3-amine (0.25 g) was stirred at 250° C. for 15 min under microwave irradiation. The obtained reaction mixture was purified by silica gel column chromatography to give the title compound as a colorless solid (0.27 g, 46%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08592431B2 |
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| Quelldatensatz | uspto-grants-2013_11 |
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| ORD ID | ord-eb57ea2519014c1f9b11941bc0b70a47 |
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| Quellennotiz | uspto-grants-2013_11 |
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