HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dibenzylhydroxylamine → N-n-Octadecyl-3-[(N,N-dibenzylamino)oxy]pyrrolidine-2,5-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dibenzylhydroxylamine | HCID 69297 | — |
| Edukt | 1-octadecyl-1H-pyrrole-2,5-dione | HCID 87118 | — |
| Produkt | N-n-Octadecyl-3-[(N,N-dibenzylamino)oxy]pyrrolidine-2,5-dione | HCID 14224083 | — |
Reaktionsschritte
The procedure of Example 1 is repeated using 6.10 g (29 mmole) of N,N-dibenzylhydroxylamine and 10.0 g (29 mmole) of N-n-octadecylmaleimide. The residue is purified by preparative HPLC (Silica gel: 9:1 heptane:ethyl acetate eluent) to give 8.0 g (49%) of a waxy solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04678826 |
| Quelldatensatz | uspto-grants-1987_07 |
| ORD ID | ord-0b85d6a48ba1415095c7ab32c6b3787b |
| Quellennotiz | uspto-grants-1987_07 |