HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Lithium amide → 5-Methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Lithium amide | HCID 24532 | — |
| Edukt | methyl 5-methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxylate | HCID 15294536 | — |
| Produkt | 5-Methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxamide | HCID 15294533 | 68% |
Reaktionsschritte
Prepared from methyl 5-methoxy-1-methyl-3-[(1-methylethyl)thio]-1H-indole-2-carboxylate and lithium amide as described in Example 23. Yield 68% after recrystallization from ethyl acetate-hexane; mp 122°-124° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05424329 |
| Quelldatensatz | uspto-grants-1995_06 |
| ORD ID | ord-a7f979b7f8b24b2c95f16e4a87726e4b |
| Quellennotiz | uspto-grants-1995_06 |