HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 3-Methylbenzoyl chloride | HCID 74375 | — |
| Edukt | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine | HCID 15294604 | — |
Reaktionsschritte
To a stirred mixture of N'-t-butyl-N'-benzoylhydrazine (1.0 g) in 15 ml toluene and aqueous sodium hydroxide (0.5 g of 50% NaOH) was added 3-toluoyl-chloride (0.9 g). After stirring for 2 hours, the product was isolated by filtration to give N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine in good yield: m.p. 111°-114° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05424333 |
| Quelldatensatz | uspto-grants-1995_06 |
| ORD ID | ord-32bba065ba434b10a71460d0eeef938b |
| Quellennotiz | uspto-grants-1995_06 |