HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Toluene → N'-t-butyl-N-(thiobenzoyl)-N'-(3-toluoyl)hydrazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Toluene | HCID 1140 | — |
| Edukt | 3-Methylbenzoyl chloride | HCID 74375 | — |
| Edukt | N'-t-butyl-N-(thiobenzoyl)hydrazine | HCID 19367775 | — |
| Katalysator | Sodium Hydroxide | HCID 14798 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | N'-t-butyl-N-(thiobenzoyl)-N'-(3-toluoyl)hydrazine | HCID 15294606 | — |
Reaktionsschritte
N'-t-butyl-N-(thiobenzoyl)hydrazine (ca. 1 g), m-toluoyl chloride (approx. 0.7 g) and 50% aqueous sodium hydroxide (6 drops) were mixed in 1 ml water and 10 ml toluene at 23° C. After stirring for 3 hours, ether-hexane was added and the product was isolated by filtration (0.25 g): m.p. 165°-168° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05424333 |
| Quelldatensatz | uspto-grants-1995_06 |
| ORD ID | ord-f6788d9e4e0e4d4f842feb17a5154dc4 |
| Quellennotiz | uspto-grants-1995_06 |