HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Azido-2-[2-(2-azidoethoxy)ethoxy]ethane → Bis-Aminoethylglycol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Azido-2-[2-(2-azidoethoxy)ethoxy]ethane | HCID 10845705 | — |
| Katalysator | Platinum | HCID 23939 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | Bis-Aminoethylglycol | HCID 70248 | — |
Reaktionsschritte
To a solution of diazide 19 (14.67 g, 0.073 mol) in THF (100 ml) 1.5 g of 5% Pt on charcoal is added. The mixture is stirred for 12 h under hydrogen. Filtration through Celite™ and evaporation of solvents at reduced pressure gives 1,8-diamino-3,6-dioxa-octane 20.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06399071B1 |
| Quelldatensatz | uspto-grants-2002_06 |
| ORD ID | ord-a477a5d3ee1340b9ac5c6b429b66c7c0 |
| Quellennotiz | uspto-grants-2002_06 |