HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Picolyl chloride hydrochloride → HCID 17854317, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Picolyl chloride hydrochloride | HCID 23392 | — |
| Edukt | 5-benzyloxy-N-(6-isopropylpyridin-3-yl)-N-[(pyrazol-4-yl)methyl]-1,2,3,4-tetrahydronaphthalene-1-carboxamide hydrochloride | HCID 67183027 | — |
| Produkt | HCID 17854317 | HCID 17854317 | 85,8% |
Reaktionsschritte
By the reaction and treatment in the same manner as in Example 271 using 5-benzyloxy-N-(6-isopropylpyridin-3-yl)-N-[(pyrazol-4-yl)methyl]-1,2,3,4-tetrahydronaphthalene-1-carboxamide hydrochloride (0.78 g) and 2-(chloromethyl)pyridine hydrochloride (0.49 g) as starting materials, 5-benzyloxy-N-(6-isopropylpyridin-3-yl)-N-{[1-(2-pyridylmethyl)pyrazol-4-yl]methyl}-1,2,3,4-tetrahydronaphthalene-1-carboxamide (0.74 g) was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08198454B2 |
| Quelldatensatz | uspto-grants-2012_06 |
| ORD ID | ord-0ce9ef2dc807492abbc2314ea5ddf17e |
| Quellennotiz | uspto-grants-2012_06 |