HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 5-(Chloromethyl)-2-methylpyrimidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | (2-Methylpyrimidin-5-yl)methanol | HCID 14686706 | — |
| Produkt | 5-(Chloromethyl)-2-methylpyrimidine | HCID 14686699 | — |
Reaktionsschritte
A solution of (2-methylpyrimidin-5-yl)methanol (95 mg, 0.77 mmol) in thionyl chloride (1 mL) was stirred at room temperature for 1 h. The mixture was concentrated to dryness and used without purification. LCMS MH+ 143.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09359359B2 |
| Quelldatensatz | uspto-grants-2016_06 |
| ORD ID | ord-2a2b5487c26648388f8b0c144ea6dbcf |
| Quellennotiz | uspto-grants-2016_06 |