HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 178490509, Verbindung → HCID 178490511, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 178490509 | HCID 178490509 | — |
| Katalysator | HCID 178418390 | HCID 178418390 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 178490511 | HCID 178490511 | 90,5% |
Reaktionsschritte
Using a solution of 1 g of N-(2-dimethylaminoethyl)-N-(cis-4-methylcyclohexyl)-4-hydroxy-3-methoxycinnamamide (Example 111) in 60 ml of methanol, and 0.05 g of 10% palladium-carbon, a reaction similar to that conducted in Example 76 was carried out. As a result, 0.91 g of N-(2-dimethylaminoethyl)-N-(cis-4-methylcyclohexyl)-3-(4-hydroxy-3-methoxyphenyl)propionamide (a compound of the present invention) was obtained as a colorless oil, which had the following physiochemical properties:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05344845 |
| Quelldatensatz | uspto-grants-1994_09 |
| ORD ID | ord-7befdfd132924a2aa4dc697ab898de5c |
| Quellennotiz | uspto-grants-1994_09 |