HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Acid → 4-Chloro-1-naphthol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Hydrogen Bromide | HCID 260 | — |
| Edukt | 1-Chloro-4-methoxynaphthalene | HCID 606038 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 4-Chloro-1-naphthol | HCID 11787 | — |
Reaktionsschritte
The known compound 1-chloro-4-methoxynaphthalene is dissolved in 150 ml. of acetic acid and 150 ml. of 48 percent hydrobromic acid, and the mixture is heated at its reflux temperature for two hours. The mixture is diluted with 200 ml. of water and cooled to provide 1-chloro-4-hydroxynaphthalene as a crystalline solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04231965 |
| Quelldatensatz | uspto-grants-1980_11 |
| ORD ID | ord-75bb562052a04de6b8ce245d5a3a77fa |
| Quellennotiz | uspto-grants-1980_11 |