HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Methylindole-2-carboxaldehyde → 3,4-Dimethyl-2-(methylaminomethyl)thieno[2,3-b]thiophene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Methylindole-2-carboxaldehyde | HCID 267164 | — |
| Edukt | 3,4-Dimethylthieno[2,3-B]Thiophene-2-Carbaldehyde | HCID 2778771 | — |
| Produkt | 3,4-Dimethyl-2-(methylaminomethyl)thieno[2,3-b]thiophene | HCID 22593756 | 53% |
Reaktionsschritte
According to the procedure of Preparation 24(a), except substituting 3,4-dimethylthieno[2,3-b]thiophene-2-carboxaldehyde (0.5 g, 2.5 mmole) for the 1-methylindole-2-carboxaldehyde, the title compound (0.28 g, 53%) was prepared as a colorless oil: MS (ES) m/e 212 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07557125B2 |
| Quelldatensatz | uspto-grants-2009_07 |
| ORD ID | ord-2ed4e6cc15e7466c85d7d1c0f3c77dbb |
| Quellennotiz | uspto-grants-2009_07 |