HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl Palmitate → HCID 10028839, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl Palmitate | HCID 8181 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 1,2-Propanediol, 3-(dodecylamino)- | HCID 102496 | — |
| Produkt | HCID 10028839 | HCID 10028839 | — |
Reaktionsschritte
N-(2,3-dihydroxypropyl)-N-dodecylamine (0.50 g, 0.0019 mole) and potassium hydroxide (0.01 g, 0.18 mmole) were heated to 85° C. under vacuum. Methyl palmitate (0.57 g, 0.0021 mole) was heated and added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off-white solid was obtained (crude yield=0.92 g) The waxy solid was recrystalized from hot hexane (yield=0.6 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05476671 |
| Quelldatensatz | uspto-grants-1995_12 |
| ORD ID | ord-b11b42c77fe640e990fcaed9891e958c |
| Quellennotiz | uspto-grants-1995_12 |