HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 1,4-Diazepan-2-one hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | tert-Butyl 3-oxo-1,4-diazepane-1-carboxylate | HCID 21962087 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | 1,4-Diazepan-2-one hydrochloride | HCID 23447544 | — |
Reaktionsschritte
Compound from Step B was treated with 4 N hydrogen chloride in dioxane at ambient temperature for 2.5 h. Concentration gave the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07560455B2 |
| Quelldatensatz | uspto-grants-2009_07 |
| ORD ID | ord-9334e80c14c045b58a60d9f0a1165788 |
| Quellennotiz | uspto-grants-2009_07 |