HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,1,3-Benzothiadiazole-4-carbaldehyde → (S)-N-(benzo[c][1,2,5]thiadiazol-4-ylmethyl)-1,1-diethoxypropan-2-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,1,3-Benzothiadiazole-4-carbaldehyde | HCID 2776283 | — |
| Edukt | (2S)-1,1-Diethoxy-2-propanamine | HCID 12398111 | — |
| Produkt | (S)-N-(benzo[c][1,2,5]thiadiazol-4-ylmethyl)-1,1-diethoxypropan-2-amine | HCID 67088326 | 95% |
Reaktionsschritte
According to the procedure described in the synthesis method of Compound IX-5, (S)-1,1-diethoxypropan-2-amine (Compound XVIII-1) (883 mg, 6.0 mmol) was reacted with benzo[c][1,2,5]thiadiazole-4-carbaldehyde (837 mg, 5.1 mmol) to obtain the title compound (1.41 g, 95%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09126981B2 |
| Quelldatensatz | uspto-grants-2015_09 |
| ORD ID | ord-e3d678c26ebd43bbbc95b8ff078d8552 |
| Quellennotiz | uspto-grants-2015_09 |